| dc.creator |
Mayoral Gastón, María del Carmen |
|
| dc.creator |
Andrés Gimeno, José Manuel |
|
| dc.creator |
Bona, M. T. |
|
| dc.creator |
Angurel, Luis A. |
|
| dc.creator |
Natividad, Eva |
|
| dc.date |
2008-05-21T09:24:01Z |
|
| dc.date |
2008-05-21T09:24:01Z |
|
| dc.date |
2004 |
|
| dc.date.accessioned |
2017-01-31T01:24:08Z |
|
| dc.date.available |
2017-01-31T01:24:08Z |
|
| dc.identifier |
Thermochimica Acta 409 (2004) 157–164 |
|
| dc.identifier |
http://hdl.handle.net/10261/4398 |
|
| dc.identifier |
10.1016/S0040-6031(03)00354-X |
|
| dc.identifier.uri |
http://dspace.mediu.edu.my:8181/xmlui/handle/10261/4398 |
|
| dc.description |
journal page:
http://www.elsevier.com/wps/find/journaldescription.cws_home/500855/description#description |
|
| dc.description |
Differential scanning calorimetry (DSC) has been used to simulate laser fusion of ceramic precursors to prepare BSCCO high temperature
superconducting materials. At fast heating rates, typical of the laser floating zone, the energy required for complete melting of the precursor
increases with the Bi to Sr+Ca ratio, in agreement with the critical current results obtained. At lowheating rates, solid-state reactions involving
ionic rearrangements take place before incongruent melting. These changes can be divided into three processes and can be quantified from
calorimetric measurements. Lower heating rates and isothermal experiments allow detailed visualisation of the ionic arrangements taking
place. The results prove that the mechanism of the final phase formation is dependent on the fabrication procedure. |
|
| dc.description |
Peer reviewed |
|
| dc.format |
658300 bytes |
|
| dc.format |
application/pdf |
|
| dc.language |
eng |
|
| dc.publisher |
Elsevier |
|
| dc.rights |
openAccess |
|
| dc.subject |
DSC |
|
| dc.subject |
BSCCO superconductors |
|
| dc.subject |
Solid diffusion |
|
| dc.subject |
Precursor composition |
|
| dc.title |
Approximation to the laser floating zone preparation of high temperature BSCCO superconductors by DSC |
|
| dc.type |
Artículo |
|